Automated Reactor

The YanZheng Fully Automatic Reactor Test System is also known as: Automated Reactor, Automated Reactor Unit, Reactor-Based Automation Equipment, or Reactor Automation Equipment. As a key component of the intelligent hydrothermal synthesis–based material preparation system, the YanZheng Fully Automatic Reactor serves as the critical link connecting catalyst preparation at the front end with analytical testing at the back end. Its primary focus is on efficiently enhancing the fully automated evaluation of catalysts and the experimentation of process parameters, thereby improving the efficiency of catalyst evaluation in slurry bed processes.

Classification:

High‑pressure reactor

Messageboard

Telephone:

400-920-1718

Product Description

The Yan Zheng fully automatic reactor test setup comprises the following four modules:
(1) Fully Automatic Slurry Bed Reactor Module: Includes four independently operated slurry bed test reactors, a reactor vessel lifting system, an automatic reactor sealing system, a reactor sealing pressure testing and pressurization system, reactor temperature control and monitoring, and is fully compatible with external automated liquid‑phase and solid‑phase feeding systems.
(2) Fully Automatic Feed Control Module: Includes liquid-phase solvent feed, gas-phase feed, rinse liquid feed, and fully automatic purging across four independent channels.
(3) Discharge and Filtration Control Module: Includes system pressure adjustment and control, system waste liquid drainage and collection, an automatic consumables replenishment system for the ultrafiltration system, a pressurized filtration system, filtrate receiving equipment, and a product reagent packaging system.
(4) Intelligent Protection and Monitoring Module: Includes external protection, an automated identification and control operation interface, hazardous gas leak alarms, and level detection alarms.
(5) Data Acquisition and Processing Information Module: Includes a process data acquisition and transmission system, as well as operational condition information acquisition and transmission; it must be equipped with reserved data interfaces for integration with other information systems, facilitating unified monitoring and management by the intelligent laboratory data management system.

Typical Experimental Procedure for the YanZheng Fully Automatic Reactor:
The experimental procedure is as follows: The supplier shall develop a detailed design plan according to the following steps (adjustments may be made if the proposed solution is superior to the current one).
1. System Verification and Parameter Tuning
a. Self‑checking of the system, sensor zeroing, power‑on checks, etc.
b. Control personnel input the required process parameters and relevant material evaluation information, then select the test plan.

2. System Feeding and Test Preparation
a. The automatic liquid‑feeding system adds a fixed volume of solvent, with the solvent volume being approximately 20 ml.
b. The reactor sealing ring retracts, the hydraulic rod returns, and the reactor sealing ring opens.
c. Exhaust the lifting cylinder of the reactor body; lower the reactor body together with the heating furnace.
d. Open the reactor vessel.
e. External solid powder is quantitatively fed via a robotic arm, with source reduction and weight calibration.
f. The diluted raw materials are quantitatively fed externally via a robotic arm, with weight calibration performed based on reduced material input.
g. The lifting cylinder for the reactor body is supplied with air, causing the reactor body and heating furnace to rise.
h. The reactor sealing ring is engaged, hydraulic rods introduce the liquid, and the reactor is fully sealed.
i. Introduce low-pressure hydrogen gas to purge and replace the contents within the reactor.
j. Introduce the feed gas into the high‑pressure system and perform a pressure‑retention test.
k. Hold pressure for 10–15 minutes and monitor the system for pressure drop.
l. If the pressure drop exceeds the specified limit and the reactor has not been properly sealed, an alarm will be triggered, and the system will vent hydrogen to atmospheric pressure, requiring manual intervention by operating personnel.
m. If the pressure drop meets the specifications, the system begins to heat up and introduce intake air, while the control system initiates stirring and reaction.

3. Evaluation of Slurry Bed Tests
a. System pressure‑controlled reaction: Set process parameters such as reaction temperature, pressure, feed rate, and stirring speed.
b. The system process records and monitors data in real time, then uploads it to the laboratory management system.
c. Alarm and emergency stop shall be triggered for abnormal parameters such as overtemperature and overpressure.
d. After the reaction is complete, the system stops heating and cools down to slightly above room temperature.
e. Release the system to atmospheric pressure and open the reactor lid.
f. Externally, a robotic arm is used to quantitatively dispense internal standards (prepared organic solvent solutions at a fixed concentration), with source reduction weighing calibration.
g. Close the reactor lid
h. Pressurize the system to 0.15–0.3 MPaG
i. Open the bottom feed valve and carry out liquid phase sampling via the bottom feed line.

4. System Cleaning and Product Filtration
a. At position #1 of the rotary fixture, first use the feeder to drop or push an empty filter cartridge into position #1.
b. The produced fluid is added to the filtration column.
c. Rotate the fixture to move the filter column that has been filled with liquid to Position 2.
d. The product test tubes are moved via a moving platform to push the selected tubes beneath the cap‑removal fixture.
e. The cap‑removal tool descends, the test tube cap is removed, and the test tube cap remains on the chuck.
f. The mobile platform pushes the open test tubes under the filtration column at position #2.
g. The piston descends, filtering and squeezing out the slurry.
h. Set the inlet pressure of the piston rod, set the differential pressure for filtration and pressurization, and extrude the filtrate.
i. Set the pressurization time and complete the pressurized filtration.
j. Piston rises
k. Rotate the filter column to position 3 and discard the filter column.
1. The bottom-insertion pipe and discharge pipeline are flushed with cleaning solution and purged with nitrogen; the waste liquid flows directly from beneath the empty space at Position #1 into the waste liquid tank.
m. The mobile platform will move the liquid‑filled test tube from beneath the filtration column at position #2 to just below the cap‑removal fixture.
n. Cap the workwear and complete sampling.
o. After completing a batch of sampling, the tube rack is moved to a designated location, where an external robotic arm removes the entire tray and places a new tube rack in its stead.

5. System Restore
a. The system performs data analysis and report generation, providing separate alerts for abnormal responses such as temperature increases or decreases, while assessing the completeness and accuracy of the experimental process to ensure the precision of product evaluation.
b. Restore the system to its original state and wait for the next operation command.

Details

Technical parameters

Product Description
Technical parameters
Product Details Chart

Details

The Yan Zheng fully automatic reactor test setup comprises the following four modules:
(1) Fully Automatic Slurry Bed Reactor Module: Includes four independently operated slurry bed test reactors, a reactor vessel lifting system, an automatic reactor sealing system, a reactor sealing pressure testing and pressurization system, reactor temperature control and monitoring, and is fully compatible with external automated liquid‑phase and solid‑phase feeding systems.
(2) Fully Automatic Feed Control Module: Includes liquid-phase solvent feed, gas-phase feed, rinse liquid feed, and fully automatic purging across four independent channels.
(3) Discharge and Filtration Control Module: Includes system pressure adjustment and control, system waste liquid drainage and collection, an automatic consumables replenishment system for the ultrafiltration system, a pressurized filtration system, filtrate receiving equipment, and a product reagent packaging system.
(4) Intelligent Protection and Monitoring Module: Includes external protection, an automated identification and control operation interface, hazardous gas leak alarms, and level detection alarms.
(5) Data Acquisition and Processing Information Module: Includes a process data acquisition and transmission system, as well as operational condition information acquisition and transmission; it must be equipped with reserved data interfaces for integration with other information systems, facilitating unified monitoring and management by the intelligent laboratory data management system.

Typical Experimental Procedure for the YanZheng Fully Automatic Reactor:
The experimental procedure is as follows: The supplier shall develop a detailed design plan according to the following steps (adjustments may be made if the proposed solution is superior to the current one).
1. System Verification and Parameter Tuning
a. Self‑checking of the system, sensor zeroing, power‑on checks, etc.
b. Control personnel input the required process parameters and relevant material evaluation information, then select the test plan.

2. System Feeding and Test Preparation
a. The automatic liquid‑feeding system adds a fixed volume of solvent, with the solvent volume being approximately 20 ml.
b. The reactor sealing ring retracts, the hydraulic rod returns, and the reactor sealing ring opens.
c. Exhaust the lifting cylinder of the reactor body; lower the reactor body together with the heating furnace.
d. Open the reactor vessel.
e. External solid powder is quantitatively fed via a robotic arm, with source reduction and weight calibration.
f. The diluted raw materials are quantitatively fed externally via a robotic arm, with weight calibration performed based on reduced material input.
g. The lifting cylinder for the reactor body is supplied with air, causing the reactor body and heating furnace to rise.
h. The reactor sealing ring is engaged, hydraulic rods introduce the liquid, and the reactor is fully sealed.
i. Introduce low-pressure hydrogen gas to purge and replace the contents within the reactor.
j. Introduce the feed gas into the high‑pressure system and perform a pressure‑retention test.
k. Hold pressure for 10–15 minutes and monitor the system for pressure drop.
l. If the pressure drop exceeds the specified limit and the reactor has not been properly sealed, an alarm will be triggered, and the system will vent hydrogen to atmospheric pressure, requiring manual intervention by operating personnel.
m. If the pressure drop meets the specifications, the system begins to heat up and introduce intake air, while the control system initiates stirring and reaction.

3. Evaluation of Slurry Bed Tests
a. System pressure‑controlled reaction: Set process parameters such as reaction temperature, pressure, feed rate, and stirring speed.
b. The system process records and monitors data in real time, then uploads it to the laboratory management system.
c. Alarm and emergency stop shall be triggered for abnormal parameters such as overtemperature and overpressure.
d. After the reaction is complete, the system stops heating and cools down to slightly above room temperature.
e. Release the system to atmospheric pressure and open the reactor lid.
f. Externally, a robotic arm is used to quantitatively dispense internal standards (prepared organic solvent solutions at a fixed concentration), with source reduction weighing calibration.
g. Close the reactor lid
h. Pressurize the system to 0.15–0.3 MPaG
i. Open the bottom feed valve and carry out liquid phase sampling via the bottom feed line.

4. System Cleaning and Product Filtration
a. At position #1 of the rotary fixture, first use the feeder to drop or push an empty filter cartridge into position #1.
b. The produced fluid is added to the filtration column.
c. Rotate the fixture to move the filter column that has been filled with liquid to Position 2.
d. The product test tubes are moved via a moving platform to push the selected tubes beneath the cap‑removal fixture.
e. The cap‑removal tool descends, the test tube cap is removed, and the test tube cap remains on the chuck.
f. The mobile platform pushes the open test tubes under the filtration column at position #2.
g. The piston descends, filtering and squeezing out the slurry.
h. Set the inlet pressure of the piston rod, set the differential pressure for filtration and pressurization, and extrude the filtrate.
i. Set the pressurization time and complete the pressurized filtration.
j. Piston rises
k. Rotate the filter column to position 3 and discard the filter column.
1. The bottom-insertion pipe and discharge pipeline are flushed with cleaning solution and purged with nitrogen; the waste liquid flows directly from beneath the empty space at Position #1 into the waste liquid tank.
m. The mobile platform will move the liquid‑filled test tube from beneath the filtration column at position #2 to just below the cap‑removal fixture.
n. Cap the workwear and complete sampling.
o. After completing a batch of sampling, the tube rack is moved to a designated location, where an external robotic arm removes the entire tray and places a new tube rack in its stead.

5. System Restore
a. The system performs data analysis and report generation, providing separate alerts for abnormal responses such as temperature increases or decreases, while assessing the completeness and accuracy of the experimental process to ensure the precision of product evaluation.
b. Restore the system to its original state and wait for the next operation command.

Product Description
Technical parameters
Product Details Chart

The Yan Zheng fully automatic reactor test setup comprises the following four modules:
(1) Fully Automatic Slurry Bed Reactor Module: Includes four independently operated slurry bed test reactors, a reactor vessel lifting system, an automatic reactor sealing system, a reactor sealing pressure testing and pressurization system, reactor temperature control and monitoring, and is fully compatible with external automated liquid‑phase and solid‑phase feeding systems.
(2) Fully Automatic Feed Control Module: Includes liquid-phase solvent feed, gas-phase feed, rinse liquid feed, and fully automatic purging across four independent channels.
(3) Discharge and Filtration Control Module: Includes system pressure adjustment and control, system waste liquid drainage and collection, an automatic consumables replenishment system for the ultrafiltration system, a pressurized filtration system, filtrate receiving equipment, and a product reagent packaging system.
(4) Intelligent Protection and Monitoring Module: Includes external protection, an automated identification and control operation interface, hazardous gas leak alarms, and level detection alarms.
(5) Data Acquisition and Processing Information Module: Includes a process data acquisition and transmission system, as well as operational condition information acquisition and transmission; it must be equipped with reserved data interfaces for integration with other information systems, facilitating unified monitoring and management by the intelligent laboratory data management system.

Typical Experimental Procedure for the YanZheng Fully Automatic Reactor:
The experimental procedure is as follows: The supplier shall develop a detailed design plan according to the following steps (adjustments may be made if the proposed solution is superior to the current one).
1. System Verification and Parameter Tuning
a. Self‑checking of the system, sensor zeroing, power‑on checks, etc.
b. Control personnel input the required process parameters and relevant material evaluation information, then select the test plan.

2. System Feeding and Test Preparation
a. The automatic liquid‑feeding system adds a fixed volume of solvent, with the solvent volume being approximately 20 ml.
b. The reactor sealing ring retracts, the hydraulic rod returns, and the reactor sealing ring opens.
c. Exhaust the lifting cylinder of the reactor body; lower the reactor body together with the heating furnace.
d. Open the reactor vessel.
e. External solid powder is quantitatively fed via a robotic arm, with source reduction and weight calibration.
f. The diluted raw materials are quantitatively fed externally via a robotic arm, with weight calibration performed based on reduced material input.
g. The lifting cylinder for the reactor body is supplied with air, causing the reactor body and heating furnace to rise.
h. The reactor sealing ring is engaged, hydraulic rods introduce the liquid, and the reactor is fully sealed.
i. Introduce low-pressure hydrogen gas to purge and replace the contents within the reactor.
j. Introduce the feed gas into the high‑pressure system and perform a pressure‑retention test.
k. Hold pressure for 10–15 minutes and monitor the system for pressure drop.
l. If the pressure drop exceeds the specified limit and the reactor has not been properly sealed, an alarm will be triggered, and the system will vent hydrogen to atmospheric pressure, requiring manual intervention by operating personnel.
m. If the pressure drop meets the specifications, the system begins to heat up and introduce intake air, while the control system initiates stirring and reaction.

3. Evaluation of Slurry Bed Tests
a. System pressure‑controlled reaction: Set process parameters such as reaction temperature, pressure, feed rate, and stirring speed.
b. The system process records and monitors data in real time, then uploads it to the laboratory management system.
c. Alarm and emergency stop shall be triggered for abnormal parameters such as overtemperature and overpressure.
d. After the reaction is complete, the system stops heating and cools down to slightly above room temperature.
e. Release the system to atmospheric pressure and open the reactor lid.
f. Externally, a robotic arm is used to quantitatively dispense internal standards (prepared organic solvent solutions at a fixed concentration), with source reduction weighing calibration.
g. Close the reactor lid
h. Pressurize the system to 0.15–0.3 MPaG
i. Open the bottom feed valve and carry out liquid phase sampling via the bottom feed line.

4. System Cleaning and Product Filtration
a. At position #1 of the rotary fixture, first use the feeder to drop or push an empty filter cartridge into position #1.
b. The produced fluid is added to the filtration column.
c. Rotate the fixture to move the filter column that has been filled with liquid to Position 2.
d. The product test tubes are moved via a moving platform to push the selected tubes beneath the cap‑removal fixture.
e. The cap‑removal tool descends, the test tube cap is removed, and the test tube cap remains on the chuck.
f. The mobile platform pushes the open test tubes under the filtration column at position #2.
g. The piston descends, filtering and squeezing out the slurry.
h. Set the inlet pressure of the piston rod, set the differential pressure for filtration and pressurization, and extrude the filtrate.
i. Set the pressurization time and complete the pressurized filtration.
j. Piston rises
k. Rotate the filter column to position 3 and discard the filter column.
1. The bottom-insertion pipe and discharge pipeline are flushed with cleaning solution and purged with nitrogen; the waste liquid flows directly from beneath the empty space at Position #1 into the waste liquid tank.
m. The mobile platform will move the liquid‑filled test tube from beneath the filtration column at position #2 to just below the cap‑removal fixture.
n. Cap the workwear and complete sampling.
o. After completing a batch of sampling, the tube rack is moved to a designated location, where an external robotic arm removes the entire tray and places a new tube rack in its stead.

5. System Restore
a. The system performs data analysis and report generation, providing separate alerts for abnormal responses such as temperature increases or decreases, while assessing the completeness and accuracy of the experimental process to ensure the precision of product evaluation.
b. Restore the system to its original state and wait for the next operation command.
技术参数
技术参数